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Creation of laboratory tasks for Selected topics from renewable energy sources and energy storage
Vaněček, Lukáš ; Vaněk, Jiří (referee) ; Bača, Petr (advisor)
This master‘s thesis contains a comprehensive laboratory task about saving a heat energy with a use of changing a state of matter. The thesis is written for the object Chosen passages of renewable resources and saving a heat energy. Part one presents a theoretical part of the topic, terminology and relations needed to make this laboratory work. It also contains a created procedure of partial tasks necessary to take laboratory measurements. The second part of the thesis is about measuring and evaluation of acquired values according to procedure described in the theoretical part of the thesis. Different variations considered during the creation of measuring procedure are also named here. The final part of the thesis describes a laboratory equipment necessary to complete the task and an example of filled protocol is attached.
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Surface tension of aqueous binary mixtures under the supercooled conditions – Development of the measuring technique and preliminary data for water + lower alcohols
Vinš, Václav ; Hykl, Jiří ; Nikl, Zbyněk ; Čenský, Miroslav ; Hrubý, Jan
An experimental apparatus originally developed for the measurement of surface tension of supercooled water was modified such that it allows for measurement of binary aqueous mixtures. The measuring principle based on the capillary rise technique is similar to that employed in the previous measurements with pure water [J. Hrubý et al., J. Phys. Chem. Lett. 5 (2014) 425 and V. Vinš et al., J. Phys. Chem. B 119 (2015) 5567]. The temperature dependence of the surface tension is determined from the\nmeasured height of the liquid column elevated in a vertical capillary tube with an inner diameter of 0.32 mm. The aqueous liquid rises to a height of 60 mm to 95 mm depending on the solute concentration and the temperature. Preliminary tests performed with the binary mixtures of water with methanol, ethanol, and n-propanol at various concentrations and temperatures down to –28 °C approved functionality of the measuring technique. Some difficulties, such as influence of impurities on the liquid column elevation or formation of bubbles in the liquid column, were observed. The experimental apparatus is further being modified in order to obtain more accurate data for various aqueous mixtures.
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Creation of laboratory tasks for Selected topics from renewable energy sources and energy storage
Vaněček, Lukáš ; Vaněk, Jiří (referee) ; Bača, Petr (advisor)
This master‘s thesis contains a comprehensive laboratory task about saving a heat energy with a use of changing a state of matter. The thesis is written for the object Chosen passages of renewable resources and saving a heat energy. Part one presents a theoretical part of the topic, terminology and relations needed to make this laboratory work. It also contains a created procedure of partial tasks necessary to take laboratory measurements. The second part of the thesis is about measuring and evaluation of acquired values according to procedure described in the theoretical part of the thesis. Different variations considered during the creation of measuring procedure are also named here. The final part of the thesis describes a laboratory equipment necessary to complete the task and an example of filled protocol is attached.
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Přechodové teplotní pole v komoře pro měření povrchového napětí podchlazených kapalin
Hrubý, Jan ; Müller, M. ; Richtr, K. ; Mareš, R.
Results of mathematical modeling of the transient temperature field in a new chamber developed to measure surface tension of supercooled liquids are presented. The chamber is designed to enable a very fast (within 0.1 s) formation of a homogeneous temperature field (within 0.02 K) after a temperature jump of 60 K. The interior of the chamber of dimensions 20x16x32 mm is filled with dry nitrogen surrounding the measuring capillary and thermometers (very fine thermocouples and RTD’s). The temperature jump is generated by switching the flow direction of the nitrogen serving as a heat transmitting fluid. To reduce the thermal boundary layer near the bottom and ceiling walls, they are made permeable and some gas is sucked out. The flow in the chamber is laminar. We compute the temperature field analytically and numerically, using the commercial software Fluent. The results indicate that the design objectives of the experimental device were met.
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